目录中文摘要..............................................................................1Abstract..............................................................................1第一章文献综述...................................................................21.1烯醚的合成.........................................21.1.1乙二醇单烯丙基醚的合成......................................21.1.2二乙二醇单烯丙基醚的合成...................................21.1.3三羟甲基二烯丙基醚的合成...................................21.1.4季戊四醇三烯丙基醚的合成...................................31.1.5烯醚的制备小结...................................................31.2烯烃的环氧化反应...................................41.2.1过氧酸法............................................................41.2.2氯醇法................................................................41.2.3过氧化氢法.........................................................51.3小结...............................................61.4论文设计思路.......................................7第二章乙二醇单缩水甘油醚的合成..........................................82.1前言...............................................82.2实验部分...........................................92.2.1实验试剂与器材...................................................92.2.2乙二醇单缩水甘油醚的制备.................................102.2.3仪器和分析表征.................................................102.2.4结果与讨论.......................................................102.3本章小结..........................................12第三章乙氧基乙基缩水甘油醚的合成.....................................133.1前言..............................................133.2实验部分..........................................143.2.1实验试剂与器材.................................................143.2.2乙二醇乙醚缩水甘油醚的制备..............................143.2.3仪器和分析表征.................................................153.2.4结果与讨论.......................................................153.3本章小结..........................................16第四章杂多酸催化过氧化氢环氧化乙二醇二烯丙基醚...............184.1.前言..............................................184.2实验部分..........................................194.2.1实验试剂与器材.................................................194.2.2催化剂的制备....................................................194.2.3催化剂的表征与讨论...........................................204.2.4乙二醇二烯丙基醚的制备....................................214.2.5产物表征与讨论.................................................214.3本章小结..........................................23结论与展望.........................................................................25参考文献............................................................................26致谢..................................................................................27中文摘要缩水甘油醚通常是指分子链中含有一个或多个三元环氧基团的化合物。这类化合物含有高活性的环氧基团，具有粘度低、稳定性好等特点。在环氧活性稀释剂、含氯化合物稳定剂、织物整理剂等方面获得广泛应用，是一类多功能多用途的化工产品。本文通过一种两步法，以简单的乙二醇为原料，与氯丙烯反应制备烯丙基醚，再通过烯烃的环氧化反应制备出缩水甘油醚。实验后期探究了一种磷钨杂多酸催化过氧化氢的方法，发现将磷钨酸与四丁基溴化铵混合制备出的催化剂，可以有效...
