PAGE \* MERGEFORMATI灯盏花素原料药中野黄芩苷的含量测定及方法学验证目 录摘要............................................................................................................................ -IIⅠ1 前言.............................................................................................................................12 材料与仪器.................................................................................................................32.1 仪器与设备..............................................................................................................32.2 试剂与试药..............................................................................................................33 灯盏花素原料药中野黄芩苷的含量测定.................................................................43.1 色谱条件的建立与验证..........................................................................................43.2 野黄芩苷含量测定方法..........................................................................................73.3 方法学验证..............................................................................................................83.4 样品的含量测定....................................................................................................164 结果...........................................................................................................................175 讨论...........................................................................................................................175.1 稀释剂的选择........................................................................................................175.2 色谱条件筛选实验中引发的思考........................................................................175.3 强降实验中的现象及思考....................................................................................186 总结...................................................................................
