目录[摘要].............................................................................................................................1[关键词].........................................................................................................................1[ABSTRACT]................................................................................................................11仪器与试剂.................................................................................................................22研究的起因.................................................................................................................23制剂中各药材的有效成份及作用分析.....................................................................34含量测定.....................................................................................................................54.1方法与结果..............................................................................................................54.1.1样品溶液的制备[14]:...........................................................................................54.2.1空白干扰试验.......................................................................................................54.2.2线性关系考察.......................................................................................................64.2.3精密度试验...........................................................................................................74.2.4稳定性试验...........................................................................................................74.2.5重复性试验...........................................................................................................74.2.6回收率试验...........................................................................................................84.2.7样品的测定[15].......................................................................................................85.讨论.............................................................................................................................9参考文献........................................................................................................................9致谢..............................................................................................................................12红白蚕石丸中柚皮苷的含量测定研究[摘要]目的:对红白蚕石丸中柚皮苷的含量进行测定,为其构建质量标准提供参考。方法:HPLC法同时测定制剂中柚皮苷的含量。结果:HPLC法测定同时测定制剂中的柚皮苷的含量,该方法更为简便灵敏,具有良好的重复性。结论:该方法可以作为红白蚕石丸的含量测定方法。[关键词]红白蚕石丸;鉴别;检查;含量测定StudyonqualitystandardofHongbaicanshipellets[Abstract]Object:TodeterminethecontentofnaringininHongbaiCanshiWan,andtoprovideareferenceforitsconstructionofqualitystandards.Method:SimultaneouslydeterminethecontentofnaringininthepreparationbyHPLC.Results:TheHPLCmethodisusedtodeterminethecontentofnaringininthepreparationatthesametime.Thismethodissimpler,moresensitive,andhasgoodrepeatability.Conclusion:ThismethodcanbeusedasamethodforthedeterminationofthecontentofHongbaiCanshiWan.[Keywords]Redandwhitesilkwormstonepills;Identify;examination;Determinationofcontent1红白蚕石丸全方由生磁石粉、白矾、炒僵蚕、法半夏、天麻、化橘红等药材组成,具有熄风镇惊,平肝安...