下载后可任意编辑醋酸甲酯羰基化合成醋酐工艺设计12024 年 5 月 29 日下载后可任意编辑安徽建筑工业学院毕 业 设 计 (论 文)专 业 化学工程与工艺 班 级 07 化工①班 学生姓名 @@@ 学 号 07206040 @@@ 课 题 50kt/a 醋酸甲酯羰基化合成醋酐工艺设计 指导老师 葛业君 6 月 6 日22024 年 5 月 29 日下载后可任意编辑摘 要醋酐是一种重要的有机化工原料,主要作为乙酰化剂,也能用作脱水剂和溶剂等。本设计经过比较现有醋酐生产乙醛氧化联产法、醋酸裂解法和醋酸甲酯羟基合成法,醋酸甲酯羟基化法较其它两种方法具有流程短,产品质量好,消耗指标低,三废排放少等优点,代表了当前醋酐生产的先进技术潮流,国外发达国家普遍采纳此技术生产醋酐。此工艺需要解决主要问题是实现 CH3COOCH3 和CO 的高效合成。设计了醋酸甲酯羰基化合成醋酐的工艺流程进并对主要设备闪蒸器进行设计。关键词: 醋酐 化工原料 羰基化 闪蒸器 醋酸甲酯12024 年 5 月 29 日下载后可任意编辑ABSTRACTVinegar anhydride is an important organic chemical raw materials, mainly as a acylation agent, and can be used as dehydrant and solvent, etc. This design by comparing existing vinegar anhydride acetaldehyde oxidation method, the joint production of acetic acid methyl acetate cracking method and hydroxyl synthesis, methyl acetate hydroxyl method is better than the other two methods have good quality of product, process short, low consumption, waste discharge index wait for few advantages, represents the current acetic anhydride was the advanced technology of production trend, widely used in developed countries as the technology production vinegar anhydride. This process needs to solve the main problem is to realize efficient synthesis CH3COOCH3 and CO. Design the methyl acetate carbonyl compounds into the process flow into the repayment period of the main equipment braising apparatus to carry on the design.22024 年 5 月 29 日下载后可任意编辑Keywords: vinegar anhydride chemical raw materi...